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Wysłany: Czw 6:39, 30 Gru 2010
Temat postu: moncler doudoune The thermal stability of porous S
The thermal stability of porous SiC ceramics
Water quenched to room temperature, measure its mechanical strength as a function of quenching temperature. Was proud of the dense sintered SiC thermal shock test, the critical temperature (by more than the flexural strength of a sharp drop) in the 200K ~ 60OK Q changes with processing conditions. In the current study, we made a B-sic porous ceramic thermal shock test, in order to estimate the thermal motor of the table i burn training dogs pregnant Results relative to the average particle sintering temperature f ℃) Time (hours) of chlorine gas density () small r ¨ rn) 1900O. 5 Ar 663.520000.5 Shi 705.02100O. 5 氲 757.519OO3. O N 675.021003.0 N 728.02 Krypton 622.2_20003.0. Sample preparation used in business-sic powder (Central Glass Co.,
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, Ltd., purity of 99.2, the average particle size of 0.4m), is balanced by the pressure inside the rubber mold after the temperature graphite furnace at 190n ~ c ~ 2100 ℃ for burning thread, the furnace is argon or ammonia atmosphere. Sintered diamond sawn products 5x2x0 ・ 3 ~ 0.5 ram the thin samples, and all with SiC abrasive particles on the glass polishing, ultrasonic cleaning in acetone and then used the thermal shock test. Some sheets by x-ray diffraction to determine the phase composition, and measured in the electron microscope, the average particle size. Table 1 lists the mean relative density of sintered samples and particle size. With the increase of sintering temperature both increased significantly. At 2100 ℃ in argon sintered samples detected trace amounts of e-SiC (6I-I). In addition, the sintering phase composition of the samples were all 13 - SIC (3c, with the Ramsdell notation) 8. Thermal shock test: thermal shock test using water quenching. Thin samples i00 ~ 900 ℃ temperature between the different heat treatment in air into the quench water 15 ℃, a group of 10 control samples into the aluminum boat roar,
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, in the heat treatment temperature for 15 minutes each. Specimen on the bending strength is measured to take three points, each point of the load to be 0.5kg, 3.30mm point size of eight specimens in each group through the collection of relevant data the calculated average intensity, the results Figure 1. Can see that the flexural strength of porous ceramics is not a sharp decrease of 16 * Hebei quench temperature ceramic increases, the torsion bending strength began almost unchanged, until it reaches a certain AT ~, I, began the decline. By Hasselman unified theory (shown in Figure 2) bending strength can be qualitatively explained this change with the AT can also be seen from Figure 1, the bending strength increases with temperature in argon and chlorine increased with the increase. This may increase as the sintering temperature,
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, relative density and average size of small dogs has increased the phenomenon is the same. Larger particles in particular will increase the connection force between the particles, so that it will enhance the strength of sinter. At a lower temperature difference when the samples sintered in nitrogen than in the bending strength of samples sintered in argon a little too much strength. Ammonia in the sintered samples, the intensity began to decrease the temperature value than the sample sintered in argon is lower (Figure 1). This may be determined by the length of the relationship between temperature and rupture of various factors. Such as the expansion coefficient, Young's modulus,
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, Poisson ratio, mixed with the argon sintering, leading to the lattice deformation of the quenched from 800 ~ 900 ℃ cold X-ray diffraction samples showed that, for oxidation, the heat treatment process of forming a small amount of SiO. The bending strength of the sample curve shown in Figure 1, (small) SiOz presence may slightly affect the bending strength. 4. Discussion: Hot motor start up, usually at a constant rate of heat passed to the hot side of thermoelectric devices,
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, at the same time spread to the cold side. This temperature is almost constant when the device is in both sides of the formation of a stable temperature gradient, you must not be subjected to large thermal shock (water quenching) when the water cooling method for the material would offend too severe a. From the perspective of ensuring the stability of the material, it is appropriate can be seen as a way station. The current study shows that even in the 800 ~ C ~ 9OO ℃ temperature difference, the bending strength of porous SiC ceramics down to 5O. Therefore, often at a relatively low stress working under the surface heat motor, and more ~ Lsic ceramics can be said to be very reliable and practical. 3 1992 1 porous SiC sample at the waist (8) Basketball gas (b) nitrogen in the sintering. Bending strength of a hardening temperature of the entire cliff 6f △ T diagram 2 (a) quantitative description of the rupture length and the United States Department of quenching Yun Yan AT (b) dense material and porous materials fracture debate two typical ways by woolen rug myeloid AT One strength of silicon translated from the U.S. Department of Zhang Gang, \ More articles related to topics:
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